酸辣椒的护绿工艺及腌制液配方优化的研究

以青辣椒为原料,采用单因素和4因素3水平正交实验,以△a~*为指标考察青辣椒浸泡前后的色泽变化,得出辣椒绿色防护的最佳条件,即在温度为40℃时, 0.3%柠檬酸和0.06%D-异抗坏血酸钠复合溶液中浸泡45 min,辣椒的绿色防护效果最好.同时通过4因素3水平正交实验,依据感官评价标准,得到了酸辣椒腌制液的最佳配方,即将8%食盐, 2%糖, 0.4%CaCl_2和8%蒜姜(1∶1)加入到pH值为3.5-4.0的腌制溶液中,即可得到风味、口感、质地优良的酸辣椒制品.     

CoPt-Co hybrid supported on amino modified SiO_2 nanospheres as a high performance catalyst for hydrogen generation from ammonia borane

CoPt-Co hybrids were successfully supported on amino modified SiO_2 nanospheres by a chemical reduction method at a temperature of 278 K.The solid carrier i.e.amino modified SiO_2,provides numerous anchoring sites for the metal nanoparticles(NPs)to improve the dispersion while reducing the size of metal NPs.The supported NPs displayed a narrow particle size distribution on the SiO_2 surface with an average diameter of 12 nm.The XRD results alongside with the binary alloy phase diagram suggest that the resulted NPs are bimetallic,composed of CoPt and amorphous Co.Among the prepared materials,the solid with the specific composition of SiO_2@Pt_(0.1)Co_(0.9)was proved to be effective catalyst for ammonia borane(AB)hydrolysis in aqueous solution.The turnover frequency(TOF)value of the supported nanocatalyst was 25.59mol_(H_2)min~(-1)·mol_M~(-1),almost twice as that of unsupported Pt_(0.1)Co_(0.9)NPs while the activation energy was 37.05 kJ mol~(-1).Furthermore,the SiO_2@Pt_(0.1)Co_(0.9)composite manifested high catalytic activity even after five cycles of reuse.     

Effects of Cr and Mo elements on the microstructures and compressive properties of the in situ (TiC_xN_y–TiB_2)/Ni cermets

In-situ(TiC_xN_y–TiB_2)/Ni cermets with 70 wt%TiC_xN_y–TiB_2 were successfully fabricated by combustion synthesis and hot pressing sintering in Ni-Ti-B_4C-BN powder systems.The microstructures,density,compressive properties,and hardness of the TiC_xN_y–TiB_2/Ni cermets with the addition of 0–8 wt%Cr/Mo to the Ni-Ti-B_4C-BN powder systems were compared and analysed.The results showed that the ceramic particles distributed uniformly in the cermets,and the size of the ceramic particles reduced with the Cr/Mo addition.Both Cr and Mo addition can improve the hardness,compressive properties,and fracture strains of the cermets.The hardness,compressive strength,and fracture strain of the(TiC_xN_y–TiB_2)/(Ni+Cr)cermets increased from 1561 HV,2.94 GPa,and 2.9%to 1864 HV,3.65 GPa,and 3.4%,respectively when the Cr content increased to 5 wt%.The hardness and compressive strength of the(TiC_xN_y–TiB_2)/(Ni+Mo)cermets increased from 1561 HV and 2.94 GPa to 1902 HV and 3.43 GPa,respectively when the Mo content increased to 8 wt%.The cermets with Cr had better compressive properties than the cermets with Mo.     

装配式地铁车站侧墙-顶板节点抗震性能试验研究

针对装配式地铁车站结构,提出了一种新型的车站顶板与侧墙连接节点.该节点通过车站侧墙顶部伸出的竖向U形钢筋与预制顶板两端伸出的水平U形钢筋搭接连接,从而实现侧墙与顶板间的内力传递.结合实际工程,设计制作了3个U形筋搭接构造形式各不相同的装配式足尺节点试件.通过拟静力试验,研究了节点试件的破坏形态、滞回性能、承载能力、变形性能以及耗能能力.结果表明,装配式节点试件的破坏形态包括U形筋弯弧内侧混凝土的局部受压破坏和侧墙剪切破坏.节点试件的位移延性系数为2.7-3.4,试件顶板端部的极限转角为1/22～1/27.增加节点中受拉钢筋的搭接长度,可以有效确保U形筋搭接连接在往复荷载作用下的有效性.     

四川蜂桶山省级自然保护区4个1hm2固定观测样地植物物种组成

为研究大巴山南麓物种组成特征,在四川蜂桶山省级自然保护区建立4个有代表性的1 hm2固定观测样地,调查并鉴定样地内胸径≥1 cm的木本植物.结果 显示:固定观测样地内有木本植物145种,共计7594株,分属39科89属.在活个体数量上,1号样地有2802株,2号样地有2041株,3号样地有1777株,4号样地有974株;在科组成上,以壳斗科和蔷薇科为主,松科和桦木科为主要优势物种,显示出大巴山南麓的植物群落组成特征;从区系上看,保护区植物以温带成分居多,并呈现出由热带成分向温带成分过渡的趋势;乔木层主要物种为华山松(Pinus armandii)、马尾松(Pinus massoniana)、杉木(Cunninghamia lanceolate)和多脉鹅耳枥(Carpinus polyneura),灌木层主要物种为绢毛木姜子(Litsea sericea)、荚蒾(Viburnum dilatatum)、马桑(Coriaria nepalensis)和猫儿刺(Ilex pernyi);样地内稀有种有37个,均为阔叶树种;从径级结构分析,马尾松属于稳定型种群,华山松属于衰退型种群,杉木、漆树(Toxicodendron vernicifluum)、红桦(Betula albosinensis)均属增长型种群.     

HPLC法测定9种饮料中阿斯巴甜含量研究

以市场中9种饮料为研究对象,探究阿斯巴甜含量测定方法.实验结果表明:流动相39％的甲醇水溶液,柱温30℃、流速0.8mL/min时,在210nm波长处存在阿斯巴甜的最大吸收峰,1-9号样品阿斯巴甜含量依次为:0.164mg/kg、0.079mg/kg、0.202mg/kg、0.00mg/kg、0.029mg/kg、0.043mg/kg、0.121mg/kg、0.063mg/kg、0.053mg/kg.实验精密度RSD值为1.233％、稳定性RSD值为0.395％、平均加标回收率为100.3％.研究为食品中阿斯巴甜含量检测提供理论参考.     

机场飞行区无人驾驶特种车辆的风险评估

 通过对机场飞行区无人驾驶特种车辆风险因素的研究，从内因和外因两个角度建立机场飞行区无人驾驶特种车辆风险评估模型。将三角函数与梯形函数相结合确定改进的白化权函数应用于层次分析（AHP）-灰色理论综合评价方法，从而对风险因素进行权重判断和综合评估，以无人驾驶行李拖车为例进行综合风险评估并对较大风险因素提出防范措施。     

利用摩擦振动理论分析带钢水平振动

在带钢轧制生产中,轧机振动是国内外许多轧钢厂都遇到问题.轧机振动易加速设备磨损,影响产品质量,导致产品出现振动纹等,有时甚至出现断裂等缺陷.研究了带钢轧制中水平振动问题,建立了力学模型,并且分析了自激振动产生机理,得出了自激振动是影响带钢表面质量主要原因.     

IMM迭代无迹Kalman粒子滤波目标跟踪算法

针对传统交互式多模型(interactive multiple model,IMM)算法跟踪机动式再入目标精度差和实时性不高的问题,提出一种交互式多模型迭代无迹Kalman粒子滤波算法.该算法在多模型滤波过程中采用改进的粒子滤波算法,通过迭代无迹Kalman滤波融入最新观测信息,进而生成粒子滤波的重要性密度分布,从而提高采样质量,改善滤波算法性能.仿真结果表明,提出的算法相对于交互式多模型粒子滤波算法具有更好的跟踪效果.该算法对提高跟踪机动式再入目标的精度与实时能力具有一定的理论意义.